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CILAS laser particle size distribution
CILAS laser - the automated auto sampler

MODELS \ range of measure
(direct access)

EcoSizer \ 0.3– 400 µm
930 \ 0.2 – 500 µm
1064 \ 0.04 – 500 µm
1180 \ 0.04 – 2500 µm
Size Expert
Accessories :
- video camera,
- autosampler,
- alcohol regenerator,
- small volume unit.

ISO 13320
21 CFR-11

FRAUNHOFER / MIE
Reference powders



 

FRAUNHOFER THEORY


Assumptions
Spherical, non-porous and opaque particles,
Diameter d > wavelength l,
Particles are distant enough from each other,
Random motion,
All the particles diffract the light with the same efficiency, regardless of.

Characteristic of the Airy shape

Characteristic of the Airy shape : 3d graph
Characteristic of the Airy shape : 2d graph

Circular,
Consisting in concentric rings I = f (a),
Spacing and size of the rings are linked to the particle size,
The fist zero angle is related to the diameter d by 1.22 l/d,
75% of the total energy is concentrated in the first lobe.

 

Principle

Principle

 

Aspect of the diffraction pattern with respect to the particle size

System
System
for a large particle
System
System
for a small particle

The observation of the diffraction pattern at finite distance is done through a lens (L) placed between the laser source and the detector

The observation of the diffraction pattern at finite distance

The diffraction patterns of particles having the same size converge at the same point whatever them location with respect to the lens,
The first zero on the detector is 1.22 lf/d where f is the focal length.


MIE THEORY

The Fraunhofer theory is applicable for large particles compared to the wavelength l (diffusion and absorption are not considered). 
For smaller particles, it is appropriate to use Mie Theory.
Mie schema
The Mie model takes into account both diffraction and diffusion of the light around the particle in its medium. 
To use the Mie model, it is necessary to know the complex refractive index of both the sample and the medium. 
This complex index has a real part, which is the standard refractive index, and an imaginary part, which represents absorption.

Complex index = m
m = a + b
a : real part
b : imaginary part

Because of the importance of this model, CILAS has crated a fast algorithm, which enables the user to get, within seconds, diffusion results using Mie theory and taking into account the complex index of the sample.

 
What’s New
 

sharpe analysing


Come and see our solutions at the following trade shows :
(for more details, click on the shows).

USA
optical International Conference & Exhibition on Advanced Ceramics & Composites
Booth 303
Daytona Beach, FL
January 20 - 21, 2009

optical TMS Annual Meeting
Booth 600
San Francisco, CA
February 16 - 18, 2009

optical Pittcon 2009
Booth 938
Chicago, IL
March 8 - 13, 2009

optical Particle Society of Minnesota
Roseville, MN
March 2009

optical Regional Refractories
St. Louis, MO
March 25 -26, 2009

optical Chicago Catalyst Show
Chicago, IL
May 12 - 14, 2009

optical National Catalyst Show
San Francisco, CA
May 14, 2009

optical Southeast Catalyst Show
Ashville, NC
June 7 - 12, 2009

optical MS&T 2009
Pittsburgh, PA
October 25 - 29, 2009

optical American Association of Pharmaceutical Scientists 2009
Los Angeles, CA
November 8 - 12, 2009

particle sharpe
granulometre